Hull 935 Mearns Road, Warminster, PA 18974, USA +1-800-523-2327 +1-215-672-7800

Hull 240 square foot production freeze dryer with door open 450 square foot production freeze dryer with sub-door for autoloading 30 square foot research and pilot freeze dryer with water jacketed chamber and door 540 square foot production freeze dryer showing autoloading of vials onto a product shelf

"Advancing Lyophilization and Freeze Drying Equipment for Over Fifty Years"

 

 
Home
Contact

Products & Capabilities
Freeze Drying Support
About Hull
Industry Links

Site Map
Privacy Policy
Terms of Use
 
SP Industries :   news | events | employment
Return to Previous Page
 

TECH TIPS   by   Dave Clayton

Your Source for Service Information


Polyol Ester Oil (POE)

All mechanical refrigeration systems now being manufactured for freeze dryer use are based on HFC refrigerants such as R507. The use of a Polyol Ester synthetic oil is the rule in R507 refrigeration systems. This oil has superior lubricating ability over the mineral oils commonly used in older CFC refrigerant systems.

1. Only POE oil should be used in a R507 system. However, not all POE oils are the same. There are a variety of POE oil types and grades and it is important to know which POE oil is in the system being serviced. Mixing incompatible POE oils may create problems and lead to compressor failure.

2. All POE oils are highly hydroscopic, they absorb moisture quickly and hold the moisture they absorb. Once absorbed, the moisture cannot be removed through system evacuation even at a vacuum pressure as low as 500 microns (millitorr). A contaminated system must be drained, flushed, and refilled.

3. It is important to prevent moisture from getting in the oil in the first place. The general recommendations for handling POE oil are to keep it in a metal container, transfer it with an oil pump, and keep the container sealed except when absolutely necessary.

4. Polyol Ester oils are good solvents. When upgrading a system from a CFC refrigerant such as R502 to a HFC refrigerant such as R507, the POE oil will readily remove any trace amounts of the mineral oil they are replacing. However, this also means seal, gasket, and electrical potting compounds must be carefully reviewed for compatability before adding the new oil.

5. POE oils are irritating to the skin and a real concern if they come in contact with your eyes. Hand and eye protection are essential when working with this oil. Be sure to read and follow the manufacturer's safety and handling advisories and the MSDS warnings and guidelines for the specific oil being used.

These technical tips are for use by qualified maintenance personnel who are familiar with their specific freeze drying equipment. These tips are intended only as general guidelines. Lyophilization equipment is frequently custom configured and some tips may not be appropriate for all freeze dryers. Always read and follow the directions of your equipment's maintenance manual. If you would like to discuss one of our tech tips, please contact Dave at 215-672-7800 ext-1376.



FTS       Genevac       Hull       National-Hotpack       VirTis       Wilmad-LabGlass